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Vol 10, No 2 (2019)
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https://doi.org/10.21122/2220-9506-2019-10-2

Measuring instruments

119-127 1329
Abstract

Compact actively Q-switched diode-pumped lasers based on Yb3+-materials are of practical importance for wide range of scientific, industrial and biomedical applications. The aim of this work was to study the Yb3+:LuAlO3 actively Q-switched laser.

One of the most promising crystalline hosts for rare-earth ions are Perovskite-like aluminate crystals. Yttrium aluminate crystal YAlO3 (YAP) is a well-known host with good thermal and mechanical properties (thermal conductivity for undoped crystal is about 11 W/m·K and about 8 W/m·K for Yb(5 at.%):YAP) similar to those of YAG. The reduction in the thermal conductivity of doped laser crystal in comparison with host materials is small in the case of ions with close atomic mass and ionic radii such as for Yb3+ and Lu3+. This feature makes LuAlO3 (LuAP) more promising host crystal for doping by Yb3+ ions in contrast to YAP especially for high output power laser systems.

 In our work, for the first time to the best of our knowledge actively Q-switching laser operation of Yb3+:LuAP single crystal was demonstrated. The maximum average output power of 4.9 W at 50 kHz pulse repetition frequency (PRF) with opt.-to-opt. efficiency of 21 % was obtained with 30 % OC transmittance. Output power as high as 3.3 W with 333 µJ-laser pulses with duration of about 11.5 ns was demonstrated at 10 kHz PRF the corresponding pulse peak power was 29 kW. 97 µJ second harmonic pulses obtained with 29 % conversion efficiency at 10 kHz PRF.

Performed investigations show high potential of Yb3+:LuAP crystals as active elements of compact diode pumped actively Q-switched lasers due to high stimulated emission cross-section (≈ 3.74·10-20 cm2) at 999.6 nm wavelength and significant reduction of heat load on the active element when pumping around 980 nm and generation around 999 nm.

128-137 2924
Abstract

Near background low dose rate measurements are important part of the environmental radiation monitoring. It is possible to fulfill energy response verification for the high sensitive dosimeters based on inorganic scintillation detectors in low energy region when creating reference X-ray fields with dose rates up to 5 µSv/h. The aim of this work was to create and study reference X-ray fields with low dose rate and narrow spectrum in the energy range from 15 to 250 keV using high-purity metal filters as a part of X-ray irradiator of AT300 X-ray calibration facility.

To determine the main characteristics of created X-ray fields highly sensitive comparators of photon radiation based on NaI(Tl) scintillation detectors was used. The comparators were developed in “ATOMTEX”. To verify comparators energy response the reference AT5350/1 dosimeter and ionization chamber TM32003 with sensitive volume 10000 cm3 were used.

Characteristics of X-ray fields that were created on the AT300 X-ray calibration facility to verify the energy response of high sensitive dosimeters based on scintillation detectors were investigated. The possibility to calibrate high sensitive dosimetric measuring instruments based on scintillation detectors in the energy range up to 250 keV in X-ray beams was shown.

138-150 1214
Abstract

The aim of this work is development of technique for synthesis of tin oxides films with various stoichiometric composition, characterized by high electrical conductivity and light transmittance in the UV and visible range of the electromagnetic spectrum, for their further application as humidity and gas sensors, as well as electrodes for electro-and photocatalytic converters.

Nonstoichiometric SnO/SnO2 /SnO2−δ films were synthesized by reactive magnetron sputtering of tin onto glass substrates in argon plasma with oxygen addition and with subsequent thermal oxidation of the formed layers in air. To change the structural, optical, and electrical properties of the films and to find out the optimal synthesis parameters, the oxygen content during the deposition process and the annealing temperature in air were varied in the range of 0–2 vol. % and of 200–450 °C, respectively. The characterization of the films was carried out using a 4-probe method for measuring the electrical resistance, X-ray diffraction, and optical spectroscopy of light transmission.

As a result of a comprehensive analysis of the structural, optical and electrical properties of the films, it was found that the optimal synthesis parameters to obtain the most transparent and conductive coatings promising for use as humidity, gas sensors and in photovoltaic devices are the following: oxygen content in argon plasma during sputtering process is ≈ 0,8–1,2 vol. %, the annealing temperature in air is ≈ 350–375 °C. In this case a polycrystalline film with high electrical conductivity and high transmittance in the visible and UV regions of the electromagnetic spectrum with prevailing of tin dioxide phase with structural defects (oxygen vacancies) is formed.

Methods of measurements, monitoring, diagnostics

151-159 962
Abstract

At the present time, developing of autonomous laser systems requires increasing of the output power of the laser sources used in composition of those systems and at the same time reducing of the energy usage in the system. The possibility of increasing output peak power of pulsed laser sources by using the method of synchronous non-coherent beam combining in ring fiber-optic delay line is considered by authors. Objective of this work was estimating energy effectiveness of laser systems, which based on this method.

General constructing method of the laser pulsed laser source with ring fiber delay line is considered, its block diagram and the general operating principle of similar systems are presented. Two versions of laser systems based on the described method of beam combining are presented: using an optical combiner and an optical switch; using fiber welding instead of a combiner and an optical switch. The graphical dependence of the energy effectiveness on the number of circulations in ring fiber-optic delay line is obtained for both versions of laser systems.

As a result of the analysis of the considered devices operation, it was shown that considered systems allow to obtain increasing the peak power of a laser pulse without increasing the power supply, also the system, that use welded fi instead of the optical combiner, has greater effi than system with optical combiner.

160-168 1061
Abstract

Angular measurements in optics of biological tissues are used for different applied spectroscopic task for roughness surface control, define of refractive index and for research of optical properties. Purpose of the research is investigation of the reflectance of biologic tissues by the ellipsoidal reflector method under the variable angle of the incident radiation.

The research investigates functional features of improved photometry method by ellipsoidal reflectors. The photometric setup with mirror ellipsoid of revolution in reflected light was developed. Theoretical foundations of the design of an ellipsoidal reflector with a specific slot to ensure the input of laser radiation into the object area were presented. Analytical solution for calculating the angles range of incident radiation depending on the eccentricity and focal parameter of the ellipsoid are obtained. Also created the scheme of image processing at angular photometry by ellipsoidal reflector.

The research represents results of experimental series for samples of muscle tissues at wavelengths 405 nm, 532 nm, 650 nm. During experiment there were received photometric images on the equipment with such parameters: laser beam incident angles range 12.5–62.5°, ellipsoidal reflector eccentricity 0.6, focal parameter 18 mm, slot width 8 mm.

The nature of light scattering by muscle tissues at different wavelengths was represented by graphs for the collimated reflection area. The investigated method allows qualitative estimation of influence of internal or surface layers of biologic tissues optical properties on the light scattering under variable angles of incident radiation by the shape of zone of incident light.

169-177 1092
Abstract

The development of new methods and high-bit instruments for measuring phase shifts of high-frequency periodic signals with high speed for radar and radionavigation tasks is an actual task. The purpose of this work is to create a new phase shift meter for high-frequency periodic signals based on the double-matching method using direct digital frequency synthesis.

On the basis of the proposed mathematical model of phase shift measurements of periodic signals by the method of double coincidence using the statistical accumulation of pulse coincidences, a functional diagram of a digital phase shift meter of periodic signals using a direct digital frequency synthesizer is developed. This allowed the implementation of an 8-bit converter phase shift signal to the code on the programmed logic integrated circuit EPM240T100C5N firm Altera.

The digital phase shift meter of periodic signals based on the double-matching method consists of two comparators, two short-wave pulse generators, a direct digital frequency synthesizer, two pulse counter control circuits, two short pulse coincidence circuits, two pulse counting circuits, four clock counters, four registers, a microcontroller and an indicator. Block diagram of a double-matching digital phase meter using direct digital sintesizer use minimal hardware logic.

In the developed phase shift meter, due to the use of the double-matching method, the time delay between signals does not depend on the period of input signals and can be found when changing the frequency of periodic pulses in wide limits. Measurement errors will be determined mainly by the duration of the pulses of coincidence. The use of statistical accumulation of pulse coincidence in the basis of the work allowed eliminating the restrictions on the duration of pulses of known non-ionic meters.

On the basis of the obtained results, a high-bit converter of phase shifts of high-frequency periodic signals into a binary code with high speed for problems of industrial tomography, radar and radionavigation can be developed.

178-184 777
Abstract

Methods of measuring delay time between periodic sequences of pulses are mostly based on the considered parameter direct measurement. The main disadvantage of this approach is the difficulty of ensuring the measurements accuracy in the noise conditions. The aim of this work was to develop a method that provides the ability to accurately measure small changes in time intervals, based on the analysis of the dynamic properties of the spectrum of the delayed measurement signals sum.

The developed method essence is to replace the insensitive registration of changes in the delay time between periodic pulses sequences, registration of changes in the parameters of the characteristic harmonic components of the spectrum of the resulting sum of these signals. In this case, only those harmonic components were taken into consideration that have a maximum sensitivity to delay time deviations and a minimum sensitivity to uncorrelated signal parameters changes.

To achieve the maximum effect, the influence of the pulse shape of periodic sequences on the measurement accuracy was investigated. Moreover, the trapezoidal form of impulses was taken as the basic as the most common, into which all other forms of impulses can be reborn (triangular, rectangular, sinusoidal, etc.).

The calculation results showed the effectiveness of the proposed method in order to reduce the measurement error of small changes in time intervals. In this case, the attenuation error coefficient compared with the existing measurement method amounted to Kwe = 4,78. Using the proposed approach opens up the possibility of improving the algorithmic support of measuring instruments in order to automate them and increase the measurements accuracy.

185-197 1147
Abstract

The study of the effects on the microvasculature of various vasoactive drugs requires appro-priate methods and equipment for determining the basic physiological parameters of small blood vessels: their internal diameter and cross-sectional area, specific density, and blood flow velocity. Therefore, the purpose of the article is to study the possibilities of improving the reliability of determining the internal diameter and cross-sectional area of the visible blood vessels of bulbar con-junctival of the eye.

A technique for obtaining digital video recordings of the bulbar conjunctiva of the eye, based on the pulse illumination of the study area, is proposed. A prototype of the equipment with a spatial resolution of 2 µm video is described, which allows to trace all visible blood vessels, including capillaries. An algorithm for stabilizing the position of a sequence of digital images of the bulbar conjunctiva relative to the first frame is discussed. It is based on the use of subpixel interpolation when searching for a global minimum of the standard deviation of the differences in brightness of the first and selected frame.

The proposed algorithms for tracing the vascular pattern and determining the internal diameter and cross-sectional area of the blood vessels are described. An original method for calculating them is proposed, which is based on determining the area and height of a cross section of a blood vessel image. The problem of verification of the obtained results is discussed.

The described approach to make it possible to create diagnostic images of the visible blood vessels of the bulbar conjunctiva, including the capillaries, with an indication of their diameters. Examples of the construction of histograms of the distribution of the internal diameter and cross-sectional area of these blood vessels are presented.

The proposed technique and hardware solutions have the prospect of being used in creating equipment for complex non-invasive diagnostics of the microvasculature and monitoring the effectiveness of treating various diseases of the cardiovascular system, since the conditions of the eye blood vessels correlate with the state of the blood vessels in other organs.

198-206 804
Abstract

The use of multivariate processing of spectral information has recently been favored due to the express nature of this method, the ease of use of mathematical packages, and the lack of the need to add chemical reagents. The aim of the work is using the methods of multivariate analysis of broadband transmission spectra to calibrate the physicochemical parameters of wines and to improve the accuracy of this calibration by selecting spectral variables.

Using the interval projection to latent structures of the transmission spectra in the range of 220– 2500 nm, the physicochemical characteristics of the varietal unblended Moldovan wine are calibrated. Interval methods of multivariate data analysis allow signifi reducing the root mean square calibration error in comparison with the broadband multivariate methods. Residual predictive deviations exceed the threshold value of 2.5 for K, Ca, Mg, oxalic, malic and succinic acids, 2,3-butylene glycol, ash and phenolic compounds for red wines and Mg, tartaric, citric and lactic acids, 2,3-butylene glycol, ash, phenolic compounds and soluble salts for white wines. These values demonstrate good calibration quality.

The application of the proposed method for calibrating the physicochemical parameters of wines makes it possible to replace traditional methods with spectral measurements, which are available not only in laboratory but also in the fi and characterized by small values of the root mean square error of calibration.

207-214 972
Abstract

In rolling fatigue tests the approach of the axes is usually measured once per cycle or for several loading cycles because of the difficulties of processing a large amount of data in multi-cycle testing. The aim of this work was the development and tests of smoothing model for measured by the SZ-01 center time series experimental data using wavelet transform.

With the help of the SZ center, the frictional moment in the roller/shaft system was measured allowing for studying the change in the coefficient of rolling resistance as a function of the level of the contact and non-contact bending load during wear-fatigue tests. Also the axes approach of the contacting bodies (roller and shaft) was measured at eight points on the raceway circumference in one cycle. This allowed studying the heterogeneity of local damages under conditions of rolling and mechano-rolling fatigue. When developing a software module for smoothing a large amount of experimental data from the test center, various methods of time series smoothing were used: moving average; exponential moving average; wavelet transform and moving average applied to the differences of the wavelet coefficients; wavelet transform and exponential moving average applied to the difference of the wavelet coefficients.

The results of numerical simulation showed that the best approximation to the original series was provided by the wavelet transform using an exponential moving average to smooth the differences between the coefficients of the wavelet transform.

The use of a software module based on this model in SZ-01 center allowed smoothing the time series characterizing the change of roller and shaft axes approach and torque.



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ISSN 2220-9506 (Print)
ISSN 2414-0473 (Online)