Application of the Thermal Diffusivity Standard for the Heat Transfer Parameter Control in Absorbing Materials
https://doi.org/10.21122/2220-9506-2023-14-3-173-178
Abstract
Metrological support creation and use of heat transfer etalons are important stages in the development of modern materials science. This is especially concerned to the emergence of new materials in the world with previously unattainable thermophysical parameters. The purpose of this work was to develop and experimentally verify the idea of joint application of the transient gratings method which is well-known in nonlinear optics and the single thermal diffusivity etalon of conventional type for the heat transfer metrological control in materials of a wide values range. The method proposed is based on thermal diffusivity etalon application as a source of calibrated optical signals that are excited in it by short laser pulses. Their lifetime is formed by the etalon thermal diffusivity and on the transient grating spatial period. The etalon linear graph of gratings lifetimes as a function of the gratings periods squared and grating lifetime of the material under study are used for the thermal diffusivity calculation. Thermal diffusivity of thin sub-surface layers of the samples under study – duraluminium, monocrystalline silicon and thermoelectric lead telluride film was measured. The results obtained are in close agreement with the reference values.
About the Author
E. V. IvakinBelarus
Nezavisimosti Ave., 4, Minsk 220030, Belarus
References
1. GOST 8.140-82. GSI. State primary standard and state verification scheme for measuring the thermal conductivity of solids from 0.1 to 5 W/(m·K) in the temperature range of 90÷500 K and from 5 to 20 W/(m·K) – in the temperature range of 300÷1100 K.
2. Kirillov VI. Metrological support of technical systems. Minsk: New knowledge Publishing; 2017. 424 p.
3. Artemyev BG. Metrology and metrological support. Minsk: FSUE "STANDARTINFORM" Publishing; 2010. 568 p.
4. Shishkin IF. Theoretical metrology. Part 2. Ensuring the uniformity of measurements: 4th ed. St. Petersburg, 2012. 240 p.
5. Sokolov NA, Sokolov AN. Multivalued measures of thermal conductivity for the range of 20–500 W/(m.K). Measuring Techniques. 2009;52(7): 751-754. DOI: 10.1007/s11018-009-9349-5
6. Zarichnyak YP, Khodunkov VP. On the feasibility of multivalued measures of thermal quantities in metrology. Izv. universities. Instrument Engineering. 2020;63: 257-263.
7. Ivakin EV, Kisialiou IG. A method for determining the thermal diffusion of solids and the device for its implementation. Euroasian patent No. 017906. The date of patent grant is April 30, 2013.
8. Sawada T, Harata A. Transient reflection grating for sub-surface analysis: GHz ultrasonic, thermal spectroscopy and imaging. Appl. Phys. A. 1995;61:263-268. DOI: 10.1007/BF01538191
9. Ivakin EV. Laser diffraction relaxmeter for the kinetics photoexcitation and study in condensed matter. Optical Journal. 2000;67:27-31.
10. Scaev P, Gudelis V, Jarasiunas K, Ivakin E, Kisialiou I, Nesladek M, Haenen K. Carrier recombination and diffusivity in monocrystalline CVD-grown and single-crystalline HPHT diamonds. Phys. Status Sol. 2012; A209.9:1744-1749. DOI: 10.1002/pssa.201200052
11. Maznev AA, Nelson KA, Rogers JA. Optical heterodyne detection of laser-induced gratings. Optics Letters. 1998;23(16):1319-1321. DOI: 10.1364/OL.23.001319
12. Kading O, Skurk H, Maznev A, Matthias E. Transient thermal gratings at surfaces for thermal characterization of bulk materials and thin films. Appl. Phys. A. 1995;61:253-261. DOI: 10.1007/BF01538190
13. Beletskii VM, Krivov GA. Aluminium alloys – composition, properties, technology, application. Reference book. KOMINTEKH Publishing, 2005.
14. Smith R. Semiconductors. Translation from English. Мir Publishing; 1982. 560 p.
15. Paraschuk T, Dashevsky Z, Woiciechowski K. Feasibility of a high stable PbTe: In semiconductor for thermoelectric energy applications. J. Appl. Phys. 2019; 125:245103. DOI: 10.1063/1.5106422
Review
For citations:
Ivakin E.V. Application of the Thermal Diffusivity Standard for the Heat Transfer Parameter Control in Absorbing Materials. Devices and Methods of Measurements. 2023;14(3):173-178. https://doi.org/10.21122/2220-9506-2023-14-3-173-178